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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871380Generated: November 2, 2026

3-Bromo-1-propanol → HCID 86755601, compound

https://huagongshe.com/reaction/1871380

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Bromo-1-propanolHCID 12308—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70003942—
ProductHCID 86755601HCID 86755601—

Reaction Steps

Prepared from compound 1 and 3-bromo-1-propanol as described for compound 8. Purified by chromatography (dichloromethane). Crystallized from diethyl ether/petroleum ether (60-95° C.). M.p. 94-97° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-2e4d4b3e5f0a46df9808296b55ab96f3
Source noteuspto-grants-2000_08