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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871383Generated: November 1, 2026

Phenacyl bromide → HCID 70003896, compound

https://huagongshe.com/reaction/1871383

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenacyl bromideHCID 6259—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70003942—
ProductHCID 70003896HCID 70003896—

Reaction Steps

Prepared from compound 1 and 2-bromoacetophenone as described for compound 8. Purified by chromatography [ethyl acetate: petroleum ether (60-80° C.)/1:3]. Crystallized from diethyl ether. M.p. 133-135° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-f60cd4ac1c6749b0b3cc529d92b70cb1
Source noteuspto-grants-2000_08