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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871385Generated: November 1, 2026

p-Chlorophenacyl bromide → HCID 70002262, compound

https://huagongshe.com/reaction/1871385

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Chlorophenacyl bromideHCID 68303—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70003942—
ProductHCID 70002262HCID 70002262—

Reaction Steps

Prepared from ω-bromo-4-chloroacetophenone and compound 1 as described for compound 8. Crystallized from methanol. M.p. 142°-144° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-9b5ef27726854a0990ab774840b9b64e
Source noteuspto-grants-2000_08