HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-2'-acetonaphthone → HCID 70001870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-2'-acetonaphthone | HCID 69179 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70003942 | — |
| Product | HCID 70001870 | HCID 70001870 | — |
Reaction Steps
Prepared from compound 1 and α-bromo-2'-acetonaphthone as described for compound 8. Purified by chromatography [ethyl acetate: petroleum ether (60°-80° C.)/1:3]. Crystallized from methanol at -20° C. M.p. 89°-90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-dd806604661747e6b49179323daaa819 |
| Source note | uspto-grants-2000_08 |