HCID 578496, compound → HCID 69814265, compound
Reaction equation
[NH:1]([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][OH:11])=[CH:5][CH:4]=1)[NH2:2].[CH3:12][O:13][C:14]1[CH:15]=[C:16]([C:22]2[C@H:31]3[C@H:26]([CH2:27][CH2:28][CH2:29][CH2:30]3)[C:25](=[O:32])N(CCO)N=2)[CH:17]=[CH:18][C:19]=1[O:20][CH3:21]>>[CH3:12][O:13][C:14]1[CH:15]=[C:16]([C:22]2[C@H:31]3[C@H:26]([CH2:27][CH:28]=[CH:29][CH2:30]3)[C:25](=[O:32])[N:1]([C:3]3[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][OH:11])=[CH:7][CH:8]=3)[N:2]=2)[CH:17]=[CH:18][C:19]=1[O:20][CH3:21]Participants
3
Procedure
Prepared from compound C and 2-(4-hydrazinophenyl)ethanol as described for compound 35. Crystallized from diethyl ether. M.p. 137°-139° C.
Workup
- customCrystallized from diethyl ether
Sources & evidence
- ORD record
- ord-5bc4e8df8ce5459f8554ef54a0535c3f
- Source dataset
- uspto-grants-2000_08
- Patent number
- US06103718
Reaction notes
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