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HRID1871404

反应详情

EQUATION

反应方程式

HRID 1871404 的结构方程式

REACTANTS

反应物

3
结构：ClCc1ccccc1
HCID7503

Benzyl chloride

C7H7Cl

结构：COc1ccc(C2=NNC(=O)[C@H]3CCCC[C@@H]23)cc1OC1CCCC1
HCID11727597

未命名化合物

结构：COc1ccc(C2=NN(Cc3ccccc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC
HCID70001660

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C2=NN(Cc3ccccc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC1CCCC1
HCID70001539

未命名化合物

PROCEDURE

实验过程

Prepared from compound 4 and benzylchloride as described for compound 78. Purified by chromatography [petroleum ether (60°-95° C.): ethyl acetate/4:1] and crystallized from petroleum ether (60°-95° C.)/ethyl acetate. M.p. 91°-92° C.

WORKUP

后处理

  1. customPurified by chromatography [petroleum ether (60°-95° C.): ethyl acetate/4:1]
  2. customcrystallized from petroleum ether (60°-95° C.)/ethyl acetate