HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → (cis)-2-Benzyl-4-(3,4-diethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | (cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70001660 | — |
| Reactant | (cis)-4-(3,4-Diethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-on | HCID 70002320 | — |
| Product | (cis)-2-Benzyl-4-(3,4-diethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70303935 | — |
Reaction Steps
Prepared from compound 7 and benzylchloride as described for compound 78. Crystallized from petroleum ether (60°-95° C.). M.p. 91°-92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-0c2e607980984c89a2bbc1a621466004 |
| Source note | uspto-grants-2000_08 |