HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyloxybenzyl chloride → (cis)-4-(3,4-Dimethoxyphenyl)-2-(4-methoxybenzyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Reactant | (cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70001660 | — |
| Product | (cis)-4-(3,4-Dimethoxyphenyl)-2-(4-methoxybenzyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70003834 | — |
Reaction Steps
Prepared from compound 1 and 4-methoxybenzylchloride as described for compound 78. Crystallized from diethyl ether. M.p. 77°-78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-158e2f7cc062421b99be44f2179a164b |
| Source note | uspto-grants-2000_08 |