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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871417Generated: November 4, 2026

2-Chlorobenzyl chloride → HCID 70002904, compound

https://huagongshe.com/reaction/1871417

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Chlorobenzyl chlorideHCID 11906—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70001660—
ProductHCID 70002904HCID 70002904—

Reaction Steps

Prepared from compound 1 and 2-chlorobenzylchloride as described for compound 78. Purified by chromatography (dichloromethane). Crystallized from petroleum ether (60°-95° C.). M.p. 101°-104° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-739b9d4d62a3437989cac357567bb6e7
Source noteuspto-grants-2000_08