HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 70002635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-(Chloromethyl)pyridinium chloride | HCID 74570 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Reactant | (cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70001660 | — |
| Product | HCID 70002635 | HCID 70002635 | — |
Reaction Steps
Prepared from compound 1 and 4-picolylchloride hydrochloride as described for compound 78, using 12 mmol of sodium hydride instead of 6 mmol. Purified by chromatography (dichloromethane). Crystallized from diethyl ether. M.p. 87°-89° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-5db02723549c4fc3a5c326e0ce5e8a2d |
| Source note | uspto-grants-2000_08 |