HCID 70002416, compound → HCID 70002882, compound

HRID 1871426Notes

Reaction equation

HRID 1871426 reaction equation
Cl.[CH:2]1(NN)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3]1.[CH3:13][O:14][C:15]1[CH:16]=[C:17]([C:23]2[C@H:32]3[C@H:27]([CH2:28][CH2:29][CH2:30][CH2:31]3)[C:26](=[O:33])[N:25](CCO)[N:24]=2)[CH:18]=[CH:19][C:20]=1[O:21][CH3:22]>>[CH3:13][O:14][C:15]1[CH:16]=[C:17]([C:23]2[C@H:32]3[C@H:27]([CH2:28][CH:29]=[CH:30][CH2:31]3)[C:26](=[O:33])[N:25]([CH:3]3[CH2:2][C:10]4[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=4)[CH2:4]3)[N:24]=2)[CH:18]=[CH:19][C:20]=1[O:21][CH3:22]

Participants

3

Reactant 2

HCID 70002416HCID 70002416, compoundHCID 86755609(cis)-4-(3,4-Dimethoxyphenyl)-2-(2-hydroxy-1-ethyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one

Product 1

HCID 70002882HCID 70002882, compound

Procedure

Prepared from compound C and 2-indanylhydrazine hydrochloride as described for compound 35. Crystallized from methanol (2x). M.p. 163°-164° C.

Workup

  1. customCrystallized from methanol (2x)

Sources & evidence

ORD record
ord-af601d4970bc43b1b73828599977df24
Source dataset
uspto-grants-2000_08
Patent number
US06103718

Reaction notes

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