HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethoxide → HCID 70002958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Reactant | (cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70001660 | — |
| Reactant | HCID 178435169 | HCID 178435169 | — |
| Product | HCID 70002958 | HCID 70002958 | — |
Reaction Steps
Prepared from compound 1 and 1-bromoethylbenzotriazole as described for compound 78, using sodium ethanolate instead of sodium hydride. Purified by chromatography [ethyl acetate:petroleum ether (60°-95° C.)/1:2]. Crystallized from methanol. M.p. 173°-178° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-859a89abd4af4a3d80f5094f1c88b072 |
| Source note | uspto-grants-2000_08 |