HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86755629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86755626 | HCID 86755626 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86755629 | HCID 86755629 | — |
Reaction Steps
A mixture of 10 g of compound 117, 10 g of phthalimide and 10 g of potassium carbonate was heated for 5 h at 100° C. in DMF. The mixture was diluted with water and extracted with ethyl acetate. The organic layer was dried over magnesium sulfate and evaporated. The residue was purified by chromatography (dichloromethane) and crystallized from ethyl acetate/ether. M.p. 104°-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-39b53e8bb4fa46288b23f23248314dfa |
| Source note | uspto-grants-2000_08 |