p-Bromobenzenesulfonyl chloride → HCID 9800931, compound

HRID 1871522Notes

Reaction equation

HRID 1871522 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8](Cl)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[NH2:12][C:13]1[CH:18]=[CH:17][C:16]([CH2:19][CH2:20][NH:21][CH:22](C(OC(C)(C)C)=O)[CH2:23][CH3:24])=[CH:15][CH:14]=1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:12][C:13]2[CH:14]=[CH:15][C:16]([CH2:19][CH2:20][NH:21][CH2:22][CH2:23][CH3:24])=[CH:17][CH:18]=2)(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7396p-Bromobenzenesulfonyl chlorideHCID 18691624HCID 18691624, compound

Product 1

HCID 9800931HCID 9800931, compound

Procedure

Using procedure 4, 4-bromobenzenesulfonyl chloride was added to 2-(4-aminophenyl)ethyl-1-(tert-butoxycarbonyl)propylamine to give the title compound as a solid, m.p. 141-143° C.

Sources & evidence

ORD record
ord-2f4fb409187b4c21ac35519ad069cbd3
Source dataset
uspto-grants-2000_08
Patent number
US06103766

Reaction notes

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