Sodium Hydroxide → HCID 54458725, compound

HRID 1871642Notes

Reaction equation

HRID 1871642 reaction equation
C1(CCC[CH:10]([CH2:14][C:15]2[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH2:23][O:24][N:25]=[C:26]([C:28]3[CH:33]=[CH:32][C:31]([C:34]4[CH:39]=[CH:38][CH:37]=[CH:36][N:35]=4)=[CH:30][CH:29]=3)[CH3:27])=[CH:17][CH:16]=2)[C:11]([OH:13])=[O:12])C=CC=CC=1.[OH-:40].[Na+]>>[O:40]([CH:10]([CH2:14][C:15]1[CH:20]=[CH:19][C:18]([O:21][CH2:22][CH2:23][O:24][N:25]=[C:26]([C:28]2[CH:33]=[CH:32][C:31]([C:34]3[CH:39]=[CH:38][CH:37]=[CH:36][N:35]=3)=[CH:30][CH:29]=2)[CH3:27])=[CH:17][CH:16]=1)[C:11]([OH:13])=[O:12])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 54395706HCID 54395706, compound

Product 1

HCID 54458725HCID 54458725, compound

Procedure

Reaction and post-treatment were carried out according to Example 18 using 1.28 g of ethyl 2-phenoxy-3-[4-[2-[[1-[4-(2-pyridyl)phenyl]ethylidene]aminoxy]ethoxy]phenyl]propionate obtained in Example 20 and 7.00 ml of a 1N aqueous sodium hydroxide solution to obtain 1.13 g of the desired compound as a crystalline powder.

Workup

  1. customReaction

Sources & evidence

ORD record
ord-77213d3ffe97460c8b864593f9e9a4d1
Source dataset
uspto-grants-2000_08
Patent number
US06103907

Reaction notes

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