Sodium Hydroxide → HCID 88065783, compound

HRID 1871643Notes

Reaction equation

[CH2:1]([CH:5]([CH2:9][C:10]1[CH:15]=[CH:14][C:13]([O:16][CH2:17][CH2:18][O:19][N:20]=[C:21]([C:23]2[CH:28]=[CH:27][C:26]([C:29]3[CH:34]=[CH:33][CH:32]=[CH:31][N:30]=3)=[CH:25][CH:24]=2)[CH3:22])=[CH:12][CH:11]=1)[C:6]([OH:8])=[O:7])[CH2:2][CH2:3][CH3:4].[OH-].[Na+:36]>>[Na+:36].[CH2:1]([CH:5]([CH2:9][C:10]1[CH:15]=[CH:14][C:13]([O:16][CH2:17][CH2:18][O:19][N:20]=[C:21]([C:23]2[CH:24]=[CH:25][C:26]([C:29]3[CH:34]=[CH:33][CH:32]=[CH:31][N:30]=3)=[CH:27][CH:28]=2)[CH3:22])=[CH:12][CH:11]=1)[C:6]([O-:8])=[O:7])[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 53779913HCID 53779913, compound

Product 1

HCID 88065783HCID 88065783, compound

Procedure

0.69 g of 2-butyl-3-[4-[2-[[1-[4-(2-pyridyl)phenyl]ethylidene]aminoxy]ethoxy]phenyl]propionic acid obtained in Example 24 was treated with 1.50 ml of 1N sodium hydroxide according to Example 20 to obtain 0.65 g of the desired compound as a powder.

Sources & evidence

ORD record: ord-cb6f44c8807448d29e4bcf1677c0ac04
Source dataset: uspto-grants-2000_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06103907

Reaction notes

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