HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54051372, compound → HCID 53921737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54051372 | HCID 54051372 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 53921737 | HCID 53921737 | 74% |
Reaction Steps
A solution of 278 mg (0.47 mmol) (R)-1 -[[3-[2-[(R)-2-tert-butoxycarbonyl-pyrrolidin-1-yl]-2-oxo-ethyl]-1,3-dibutyl-ureido]-acetyl]-pyrrolidine-2-carboxylic acid tert-butyl ester in 2 ml trifluoroacetic acid was stirred for 4 h at room temperature. The solvent was removed in vacuo and the residue was dried to give 167 mg (74%) of the title compound as brown foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103910 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-54712485a76c45de8c617563a5636d14 |
| Source note | uspto-grants-2000_08 |