HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Vinylbenzoic acid → 4-Vinylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Vinylbenzoic acid | HCID 14098 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Vinylbenzoyl chloride | HCID 11052028 | — |
Reaction Steps
p-vinyl benzoic acid (10 g, 0.067 mole) is suspended in benzene (25 ml). Oxalyl chloride (25 g, 0.2 mole) is added. The mixture is stirred for 8 hours under argon atmosphere. Solvent and excess oxalyl chloride is removed in vacuo. The product is distilled in vactio to yield p-vinyl benzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06106820 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-7686540c073b4dfeb95e1b3fc424db34 |
| Source note | uspto-grants-2000_08 |