HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 86755647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 86755646 | HCID 86755646 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86755647 | HCID 86755647 | — |
Reaction Steps
A mixture of the product from step (v) (1.84 g) and Lawesson's reagent (1.65 g) in 1,4-dioxane (30 ml) was heated at reflux for 24 hours. The mixture was partitioned between ethyl acetate and aqueous sodium bicarbonate. The organic phase was dried (MgSO4) and evaporated. Purification was by chromatography eluting with 50% ethyl acetate in isohexane. Yield 1.38 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107297 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-53bd5d02dd0f4b8486689564fd6dbf3e |
| Source note | uspto-grants-2000_08 |