Glycine, N-[(1,1-dimethylethoxy)carbonyl]-N-methyl- → HCID 86755656, compound
Reaction equation
C(OC([N:8]([CH2:10][C:11]([OH:13])=O)[CH3:9])=O)(C)(C)C.[CH2:14]([O:16][C:17](=[O:25])[CH2:18][C:19]1[N:20]=[C:21]([NH2:24])[S:22][CH:23]=1)[CH3:15]>>[CH3:9][NH:8][CH2:10][C:11]([NH:24][C:21]1[S:22][CH:23]=[C:19]([CH2:18][C:17]([O:16][CH2:14][CH3:15])=[O:25])[N:20]=1)=[O:13]Participants
3
Procedure
The subtitle compound was prepared from N-tert-butoxycarbonyl sarcosine (6.0 g) and 2-amino-4-thiazoleacetic acid ethyl ester (6.6 g) by the method of example 10 step (i). Yield 5.24 g
Sources & evidence
- ORD record
- ord-6dbc4d7d8576489b9eb71cab2c6c9501
- Source dataset
- uspto-grants-2000_08
- Patent number
- US06107297
Reaction notes
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