4,6-Dichloropyrimidine → HCID 18689723, compound

Participants

Reaction Steps

The subtitle compound was prepared from the product of step (ii) (0.33 g) and 4,6-dichloropyrimidine (0.149 g) by the method of example 16 step (i). Purification was by chromatography eluting with 30% ethyl acetate in isohexane. Yield 0.23 g. 1H NMR: δ (DMSO) 8.98(d,1H), 8.24(d,1H), 7.61(d,1H), 7.53(d,2H), 7.24(d,2H), 7.23(s,2H), 6.95(s,2H), 5.41(s,1H), 2.42(s,3H), 2.30(s,6H).

Provenance & Evidence