m-Xylyl bromide → HCID 22117258, compound

HRID 1872003Notes

Reaction equation

HRID 1872003 reaction equation
[CH3:1][C:2]1([CH3:17])[CH2:6][O:5][C:4]([C:7]2[CH:12]=[CH:11][C:10]([CH:13]([CH3:15])[CH3:14])=[CH:9][C:8]=2[CH3:16])=[N:3]1.Br[CH2:19][C:20]1[CH:21]=[C:22]([CH3:26])[CH:23]=[CH:24][CH:25]=1>>[CH3:17][C:2]1([CH3:1])[CH2:6][O:5][C:4]([C:7]2[CH:12]=[CH:11][C:10]([CH:13]([CH3:14])[CH3:15])=[CH:9][C:8]=2[CH2:16][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[C:22]([CH3:26])[CH:21]=2)=[N:3]1

Participants

3

Reactant 2

HCID 12099m-Xylyl bromideHCID 22117266HCID 22117266, compound

Product 1

HCID 22117258HCID 22117258, compound

Procedure

The subtitle compound was prepared from the product of step (ii) and 3-bromomethyltoluene (9.25 g) using the method of example 15 step (iv). Purification was by chromatography eluting with toluene. Yield 4.8 g.

Workup

  1. customPurification
  2. washeluting with toluene

Sources & evidence

ORD record
ord-c28b4b04cef34b4e9228005c49cf90f6
Source dataset
uspto-grants-2000_08
Patent number
US06107297

Reaction notes

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