Glycine, N-[(1,1-dimethylethoxy)carbonyl]-N-methyl- → HCID 86755660, compound

HRID 1872010Notes

Reaction equation

HRID 1872010 reaction equation
C(O[C:6]([N:8]([CH2:10][C:11](O)=[O:12])C)=O)(C)(C)C.[NH2:14][C:15]1[S:16][CH:17]=[C:18]([C:20](=[N:26][O:27][CH3:28])[C:21]([O:23][CH2:24][CH3:25])=[O:22])[N:19]=1>>[CH3:6][NH:8][CH2:10][C:11]([NH:14][C:15]1[S:16][CH:17]=[C:18]([C:20](=[N:26][O:27][CH3:28])[C:21]([O:23][CH2:24][CH3:25])=[O:22])[N:19]=1)=[O:12]

Participants

3

Reactant 2

HCID 83692Glycine, N-[(1,1-dimethylethoxy)carbonyl]-N-methyl-HCID 581091Ethyl 2-(2-aminothiazol-4-yl)-2-methoxyiminoacetate

Product 1

HCID 86755660HCID 86755660, compound

Procedure

The subtitle compound was prepared from N-[tert-butoxycarbonyl]sarcosine (2.00 g) and ethyl 2-amino-alpha-[methoxyimino]-4-thiazoleacetate (2.66 g) by the method of example 10 step (i).Yield 2.77 g.

Sources & evidence

ORD record
ord-3a50dd9c60f9499ebeafd12891cc99b0
Source dataset
uspto-grants-2000_08
Patent number
US06107297

Reaction notes

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