HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycolaldehyde dimer → HCID 10503421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycolaldehyde dimer | HCID 186078 | — |
| Reactant | 153624-15-8 | HCID 9908909 | — |
| Solvent | Dichloromethane ethylacetate | HCID 21226138 | — |
| Product | HCID 10503421 | HCID 10503421 | — |
Reaction Steps
The title compound was prepared from the compound of Example 32 and glycolaldehyde dimer as described for Example 58, with stirring at room temperature for 2 hours. Following workup, chromatography on silica gel with 4:1 methylene chloride/ethyl acetate afforded the title compound as a white solid, mp 45-53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107320 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-05dd7b514f3a49a8b08a1b1f6cfc635e |
| Source note | uspto-grants-2000_08 |