HRID1872117

反应详情

EQUATION

反应方程式

HRID 1872117 的结构方程式

PROCEDURE

实验过程

4-Methoxymethoxy-piperidine (1.0 mmol) and 2-[(5-chloro-1H-indole-2-carbonyl)-amino]-3-phenyl-propionic acid (1.0 mmol) were coupled according to Procedure A and the product purified by chromatography on silica gel eluted with 1:1 ethyl acetate-hexanes: Yield 241 mg, 50%; HPLC (60/40) 7.67 minutes (94%);

WORKUP

后处理

  1. customthe product purified by chromatography on silica gel
  2. washeluted with 1:1 ethyl acetate-hexanes
  3. customHPLC (60/40) 7.67 minutes (94%)