HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1872169Generated: November 1, 2026
HCID 7201349, compound → HCID 13689667, compound
https://huagongshe.com/reaction/1872169
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 7201349 | HCID 7201349 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 13689667 | HCID 13689667 | — |
Reaction Steps
(R)-(1-Methylcarbamoyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester (722 mg, 2.6 mmol) was dissolved in 4M HCl-dioxane (10 mL) at 0° C. The mixture was stirred for 1 hour at 25° C., concentrated and the residue triturated with ether. Yield, 517 mg, 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06107329 |
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| Source dataset | uspto-grants-2000_08 |
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| ORD ID | ord-628bb504a90444528436ac6e09e761f6 |
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| Source note | uspto-grants-2000_08 |
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