Ethyl 2-oxocyclohexanecarboxylate → HCID 9905493, compound
Reaction equation
C(OC(C1C(=O)CCCC1)=O)C.[OH:13][NH:14][C:15]([C@H:17]1[C@@H:23](CC2C=CC=CC=2)[CH2:22][CH2:21][CH2:20][CH2:19][N:18]1[S:31]([C:34]1[CH:39]=[CH:38][C:37]([O:40][CH3:41])=[CH:36][CH:35]=1)(=[O:33])=[O:32])=[O:16]>>[CH3:41][O:40][C:37]1[CH:38]=[CH:39][C:34]([S:31]([N:18]2[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH:17]2[C:15]([NH:14][OH:13])=[O:16])(=[O:32])=[O:33])=[CH:35][CH:36]=1Participants
3
Procedure
1-(4-Methoxybenzenesulfonyl)-azepane-2-hydroxamic acid was synthesized from 6-oxo-cyclohexane carboxylic acid ethyl ester in the same manner as the procedures used for the preparation of cis-3-Benzyl-1-(4-methoxybenzene sulfonyl)-azepane-2-carboxylic acid-hydroxyamide.
Sources & evidence
- ORD record
- ord-adc89fdbaa8442619ce4b7d2203f5040
- Source dataset
- uspto-grants-2000_08
- Patent number
- US06107291
Reaction notes
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