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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1872251Generated: November 1, 2026

3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-azepane-2-carboxylic acid → 1-(4-Methoxy-benzenesulfonyl)-3-phenylsulfanylmethyl-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid

https://huagongshe.com/reaction/1872251

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-azepane-2-carboxylic acidHCID 18689641—
Reactant1-(4-Methoxy-benzenesulfonyl)-3-phenylsulfanylmethyl-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid tert-butyl esterHCID 54009864—
Product1-(4-Methoxy-benzenesulfonyl)-3-phenylsulfanylmethyl-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acidHCID 54547846—

Reaction Steps

1-(4-Methoxy-benzenesulfonyl)-3-phenylsulfanylmethyl-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid was synthesized from 1-(4-Methoxy-benzenesulfonyl)-3-phenylsulfanylmethyl-2,3,4,7-tetrahydro-1H-azepine-2-carboxylic acid tert-butyl ester in the same manner as the procedures used for the preparation of 3-Acetoxymethyl-1-(4-methoxy-benzenesulfonyl)-azepane-2-carboxylic acid: MS (M-H)- =432.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06107291
Source datasetuspto-grants-2000_08
ORD IDord-2c74210b6d04446db467633958240d7b
Source noteuspto-grants-2000_08