Thionyl Chloride → HCID 18417664, compound

HRID 1872332Notes

Reaction equation

[Cl:1][CH2:2][CH2:3][CH2:4][CH2:5][CH:6](O)[CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.S(Cl)([Cl:17])=O>>[Cl:17][CH:6]([CH2:5][CH2:4][CH2:3][CH2:2][Cl:1])[CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 18690427HCID 18690427, compound

Product 1

HCID 18417664HCID 18417664, compoundYield 99.5%

Procedure

By operating as in Preparation 7 and starting from 12.3 g of 6-chloro-1-phenyl-hexan-2-ol and 12.9 g of thionyl chloride, 13.3 g of expected product is recovered.

Workup

customBy operating as in Preparation 7

Sources & evidence

ORD record: ord-9643ae6b49864be29179467a0acd9675
Source dataset: uspto-grants-2000_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06107495

Reaction notes

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