HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-[4-(4-pentylphenyl)phenyl]acrylate → Methyl 3-[4-(4-pentylphenyl)phenyl]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-[4-(4-pentylphenyl)phenyl]acrylate | HCID 54407370 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Methyl 3-[4-(4-pentylphenyl)phenyl]propionate | HCID 21182420 | 95.9% |
Reaction Steps
A mixture of Methyl 3-[4-(4-pentylphenyl)phenyl]acrylate (2.0 g) and 10% palladium on carbon (50% wet, 0.2 g) in tetrahydrofuran (20 ml) was stirred for 8 hours under atmospheric pressure of hydrogen at ambient temparature. The catalyst was filtered off, and the filtrate was evaporated under reduced pressure to give Methyl 3-[4-(4-pentylphenyl)phenyl]propionate (1.93 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107458 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-21ef4184134043f89e2349c679918704 |
| Source note | uspto-grants-2000_08 |