HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-(Hexyloxy)benzohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Methyl 4-hexyloxybenzoate | HCID 3576592 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(Hexyloxy)benzohydrazide | HCID 1625940 | 98% |
Reaction Steps
A solution of Methyl 4-n-hexyloxybenzoate (2.00 g) and hydrazine hydrate (4.24 g) in ethanol (10 ml) was refluxed for 6 hours. After cooling, the reaction mixture was poured into water. The precipitate was collected by filtration, washed with water and dried over P2O5 under reduced pressure to give N-(4-n-hexyloxybenzoyl)hydrazine (1.96 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06107458 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-810335e472294ddcbde2ae137bdc4b57 |
| Source note | uspto-grants-2000_08 |