Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Product | 4-Hydroxybenzoic Acid | HCID 135 | 10% |
Reaction Steps
Using apparatus 4, 10.3 g of KF and 4.3 g phenol were added to apparatus 4. The reactor was pressurized to 114 bar with CO2, the stirrer was set to 800 rpm, and heated at 120° C. for 86 h. Analysis by method 2 showed a yield of 10% PHBA and 5% SA.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06107516 |
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| Source dataset | uspto-grants-2000_08 |
|---|
| ORD ID | ord-158bed64a1a24c3199ef1cfc4ebd4ff6 |
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| Source note | uspto-grants-2000_08 |
|---|
