HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15840442, compound → HCID 15840443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15840442 | HCID 15840442 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15840443 | HCID 15840443 | — |
Reaction Steps
A solution of 2-(imidazol-1-yl)-6-methyl-4-(3-nitrobenzylamino)thieno[2,3-d]pyrimidine in methanol is hydrogenated in the presence of Raney nickel. The catalyst is filtered off and the solution is concentrated. After recrystallization, 2-(imidazol-1-yl)-6-methyl-4-(3-aminobenzylamino)thieno[2,3-d]pyrimidine is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06110920 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-3e811faa4c6b44fe89334f87629386e5 |
| Source note | uspto-grants-2000_08 |