Ammonia → 3-(Tridecylamino)propionamide

HRID 1872798Notes

Reaction equation

HRID 1872798 reaction equation
[CH2:1]([NH:14][CH2:15][CH2:16][C:17]([O:19]C)=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[NH3:21]>>[CH2:1]([NH:14][CH2:15][CH2:16][C:17]([NH2:21])=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 18687169Methyl 3-tridecylaminopropionate

Product 1

HCID 186872443-(Tridecylamino)propionamide

Procedure

A solution of methyl 3-(tridecylamino)propionate (0.77 g) in 10N-methanolic ammonia (7 ml) was allowed to stand at room temperature for 7 days. The resultant crystal was collected by filtration and washed with a small portion of methanol to give 3-(tridecylamino)propionamide (0.16 g).

Workup

  1. filtrationThe resultant crystal was collected by filtration
  2. washwashed with a small portion of methanol

Sources & evidence

ORD record
ord-5019b1eefeff4ea1a2e544b5029cc1d9
Source dataset
uspto-grants-2000_08
Patent number
US06110933

Reaction notes

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