Methyl 2-hydroxy-3-phenylpropanoate → HCID 9808144, compound

HRID 1872862Notes

Reaction equation

HRID 1872862 reaction equation
[Br:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12]([C:14]3[C:18]4[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=4[O:16][C:15]=3[CH2:23][CH2:24][CH2:25][CH3:26])=[O:13])=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[OH:27].C[O:29][C:30](=[O:40])[CH:31]([CH2:33][C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1)O>>[Br:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12]([C:14]3[C:18]4[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=4[O:16][C:15]=3[CH2:23][CH2:24][CH2:25][CH3:26])=[O:13])=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[O:27][CH:31]([CH2:33][C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1)[C:30]([OH:40])=[O:29]

Participants

3

Reactant 2

HCID 518800Methyl 2-hydroxy-3-phenylpropanoateHCID 10526273HCID 10526273, compound

Product 1

HCID 9808144HCID 9808144, compound

Procedure

The title compound was prepared from 1-bromo-6-(2-butyl-benzofuran-3-carbonyl)-naphthalen-2-ol, and 3-phenyllactic methyl ester, in substantially the same manner, as described in Example 5, and was obtained as a white solid, mp 165-167° C.; MS m/e 570 (M+);

Workup

  1. customwas obtained as a white solid, mp 165-167° C.

Sources & evidence

ORD record
ord-c0e2e9950c5f4d628cf381b5bb07e42c
Source dataset
uspto-grants-2000_08
Patent number
US06110963

Reaction notes

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