Stearic Acid → Octadecanoic acid, silver(1+) salt (1:1)

HRID 1873298Notes

Reaction equation

HRID 1873298 reaction equation
[C:1]([OH:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[OH-].[Na+].[N+]([O-])([O-])=O.[Ag+:27]>O>[C:1]([O-:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Ag+:27]

Participants

5

Reactant 3

HCID 5281Stearic AcidHCID 14798Sodium HydroxideHCID 24470Silver Nitrate

Product 1

HCID 160695Octadecanoic acid, silver(1+) salt (1:1)

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

7.5 g of stearic acid and 1.2 g of sodium hydroxide were added to 300 ml of water and sufficiently stirred until they were completely dissolved. 5.2 g of silver nitrate was added thereto, and the result was stirred for 3 hours. White powder on the surface of the result was collected and washed three times each with distilled water and with methanol to obtain silver stearate. An anode active material was prepared as in Example 1, except that silver stearate was used instead of nickel stearate, the molar ratio of silver to silicon was 0.2:1, the weight ratio of silicon to graphite was 0.5:1, and the carbon layer was 5.2 wt % of the anode active material.

Workup

  1. dissolutionwere completely dissolved
  2. stirringthe result was stirred for 3 hours
  3. customWhite powder on the surface of the result was collected
  4. washwashed three times each with distilled water

Sources & evidence

ORD record
ord-118de9a10e8743beb8e2aa4830d270e5
Source dataset
uspto-grants-2012_11
Patent number
USRE043794E1

Reaction notes

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