Tetrabutylammonium Fluoride → HCID 59161022, compound

Participants

Reaction Steps

4.04 g (8.91 mmol) of the compound from Example 21A are dissolved in 69 ml of dry THF, and 9.8 ml (9.8 mmol) of a 1 M solution of tetrabutylammonium fluoride in THF are added. The reaction mixture is stirred at RT for 48 h. The solvent is then removed on a rotary evaporator and the residue is purified chromatographically on silica gel 60 (mobile phase: gradient dichloromethane/ethanol 200:1→1:1).

Provenance & Evidence