Tetrabutylammonium Fluoride → HCID 59160971, compound

Participants

Reaction Steps

6.38 g (14.06 mmol) of the crude product from Example 26A are dissolved in 108 ml of dry THF, and 4.04 g (15.47 mmol) of tetra-n-butylammonium fluoride are added. The reaction mixture is stirred at RT for 48 h. After removal of the solvent the residue is directly purified chromatographically on silica gel 60 (mobile phase: gradient dichloromethane/ethanol 20:1→1:1).

Provenance & Evidence