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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1873612Generated: November 4, 2026

Sodium Bicarbonate → HCID 68734869, compound

https://huagongshe.com/reaction/1873612

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium BicarbonateHCID 516892—
ReactantMethyl 3-(bromomethyl)benzoateHCID 517981—
ReactantHCID 24959791HCID 24959791—
ReactantHCID 178510475HCID 178510475—
SolventDimethylformamideHCID 6228—
ProductHCID 68734869HCID 68734869—

Reaction Steps

140 mg (0.54 mmol) of the compound from Example 33A, 137 mg (0.60 mmol) of methyl 3-(bromomethyl)benzoate and 182 mg (2.17 mmol) of sodium bicarbonate in 2.0 ml of dry DMF are reacted analogously to the preparation of the compound of Example 29.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08304412B2
Source datasetuspto-grants-2012_11
ORD IDord-daaf3c36d5514e2c9e987cf6c7c2c024
Source noteuspto-grants-2012_11