HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 66916353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 66916250 | HCID 66916250 | — |
| Reactant | HCID 86650697 | HCID 86650697 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Methanol tetrahydrofuran water | HCID 21892291 | — |
| Product | HCID 66916353 | HCID 66916353 | — |
Reaction Steps
Similar to the synthesis of compound 1c, from compound 48a (111 mg), a mixture of water-methanol-tetrahydrofuran (1:1:1) (5 mL), iron powder (49.7 mg), and ammonium chloride (111 mg), compound 48b was yielded as a crude product (31.2 mg, yield: 31%). ESI-MS m/z 359, 361 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304427B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-674474cc1538456aab56a58a3517a4ca |
| Source note | uspto-grants-2012_11 |