Hydrazine hydrate (1:1) → HCID 53437222, compound

Participants

Reaction Steps

Next, 13.60 mmol of 4-nitro-N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline, 0.22 of 10% Pd/C, and 150 ml of ethanol were added into a bottle. Next, the mixture was heated to reflux, and 7 ml of hydrazine monohydrate was added slowly to the mixture from a dropping funnel over a period of 1 hrs under dry nitrogen. After a further 12 hrs of reflux, the mixture solution was filtered to remove Pd/C, and the filtrate was cooled to precipitate. The crude product was collected by filtration and recrystallization from ethanol to afford 4-Amino-N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline as a white crystal with a yield of 80%. The 4-amino-N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline had a melt point of 95° C.

Provenance & Evidence