Methacrolein → HCID 87290873, compound

HRID 1874086Notes

Reaction equation

HRID 1874086 reaction equation
O=[CH:2][C:3](=[CH2:5])[CH3:4].[C:6]([O:10][C:11](=[O:14])[NH:12][NH2:13])([CH3:9])([CH3:8])[CH3:7]>>[C:6]([O:10][C:11]([NH:12]/[N:13]=[CH:4]/[C:3]([CH3:5])=[CH2:2])=[O:14])([CH3:9])([CH3:8])[CH3:7]

Participants

3

Reactant 2

HCID 6562MethacroleinHCID 70091tert-Butyl carbazate

Product 1

HCID 87290873HCID 87290873, compound

Procedure

B-23a is prepared analogously to B-19a starting from methacroleine (1.18 ml, 14.3 mmol) and tert-butylcarbazate (1.89 g, 14.3 mmol). Yield: 2.61 g.

Workup

  1. customB-23a is prepared analogously to B-19a

Sources & evidence

ORD record
ord-4ceaa38258dc49f6ac71ad93e6b6fb88
Source dataset
uspto-grants-2012_11
Patent number
US08304556B2

Reaction notes

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