HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanatoformate → HCID 57749243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Reactant | HCID 57749194 | HCID 57749194 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 57749243 | HCID 57749243 | 57.9% |
Reaction Steps
In the same manner as in Reference Example 30 and using tert-butyl {5-[(6-aminopyridin-3-yl)oxy]-2-methylphenyl}carbamate (17.5 g, 44.5 mmol), DMSO (100 mL) and ethyl isothiocyanatoformate (6.50 mL, 55.0 mmol) as starting materials, the title compound (11.5 g, 49%) was obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08304557B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-8465353486be4def9d39f290611d4b75 |
| Source note | uspto-grants-2012_11 |