HCID 18149883, compound → HCID 57749155, compound

Participants

Reaction Steps

To a solution of methyl 3-[(5-nitropyridin-2-yl)oxy]benzoate (14.4 g, 52.5 mmol) in methanol (100 mL) was added palladium carbon (50% water-containing product, 1.40 g), and the mixture was stirred under a hydrogen atmosphere at room temperature for 6 hr. The reaction mixture was filtered through celite, and the filtrate was concentrated under reduced pressure, and the residue was dried to give the title compound (12.9 g, quant.) as a yellow oil.

Provenance & Evidence