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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1875586Generated: October 31, 2026

2,4-Dibromo-1-(2-bromoethoxy)benzene → HCID 11563691, compound

https://huagongshe.com/reaction/1875586

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,4-Dibromo-1-(2-bromoethoxy)benzeneHCID 12725188—
Reactant1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanolHCID 23992385—
SolventAcetonitrileHCID 6342—
ProductHCID 11563691HCID 1156369152.6%

Reaction Steps

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0557 g, 0.190 mmol) and 2-bromoethyl 2,4-dibromophenyl ether (0.110 g, 0.306 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0525 g, 43.8%). EI-MS m/z 572 (M+) Rt (2.26 min).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08309572B2
Source datasetuspto-grants-2012_11
ORD IDord-c6c4c45828a54c1d963389de6be0aa39
Source noteuspto-grants-2012_11