HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 67049825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 2-Bromo-4-chlorobenzoic acid | HCID 33126 | — |
| Reactant | 3-[2-(4-Chloro-2-cyclopentylmethoxy-phenyl)-5,6-difluoro-benzoimidazol-1-ylmethyl]-benzoic acid | HCID 58209276 | — |
| Product | HCID 67049825 | HCID 67049825 | — |
Reaction Steps
The title compound was prepared in analogy to Example 19, intermediate c, from benzene-1,2-diamine (CAS Reg. No. 76179-40-3) and 2-bromo-4-chloro-benzoic acid (CAS Reg. No. 936-08-3). Light yellow solid (92%). MS (Turbo Spray): m/z=308.8 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309581B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-167bd58920d44215b9442017351749ad |
| Source note | uspto-grants-2012_11 |