HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylaniline → N-(4-Ethylphenyl)-2-methylquinazolin-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylaniline | HCID 11504 | — |
| Reactant | 4-Chloro-2-methylquinazoline | HCID 2785421 | — |
| Product | N-(4-Ethylphenyl)-2-methylquinazolin-4-amine | HCID 42625917 | — |
Reaction Steps
The title compound was prepared from 4-chloro-2-methyl-quinazoline (100 mg, 0.56 mmol), 4-ethyl-phenylamine (0.07 ml, 0.56 mmol) by a procedure similar to Example 78. 1H NMR (CDCl3): 7.85-7.78 (m, 2H), 7.76-7.71 (m, 3H)), 7.49 (t, J=7.5 Hz, 1H), 7.36 (brs, 1H), 7.24 (s, 2H), 2.70-2.69 (m, 5H), 1.26 (t, J=7.5 Hz, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309562B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-1fcdb7136d5f4579b1a6782331facebb |
| Source note | uspto-grants-2012_11 |