(2-Bromoethyl)cyclohexane → HCID 25194458, compound

HRID 1876266Notes

Reaction equation

HRID 1876266 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([C:7](=[O:13])[C:8](=[O:12])[NH:9]2)=[CH:5][CH:4]=1.Br[CH2:15][CH2:16][CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1>>[CH:17]1([CH2:16][CH2:15][N:9]2[C:10]3[C:6](=[CH:5][CH:4]=[C:3]([O:2][CH3:1])[CH:11]=3)[C:7](=[O:13])[C:8]2=[O:12])[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1

Participants

3

Reactant 2

HCID 15440(2-Bromoethyl)cyclohexaneHCID 103749726-Methoxyisatin

Product 1

HCID 25194458HCID 25194458, compound

Procedure

The title compound was prepared as a red solid, using 6-methoxy-isatin prepared as described in Pavlidis et al. and 1-Bromo-2-cyclohexylethane following Method B. Pavlidis, V. H., et al., The Synthesis of a Novel Series of Substituted 2-Phenyl-4H-3,1-benzoxazin-4-ones, Synthetic Communications, 1994, 24:4, 533-548.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-3b2c61bfe6384ceba8090f20ee3297eb
Source dataset
uspto-grants-2012_11
Patent number
US08309595B2

Reaction notes

Loading…