HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetic acid, hydrazide → HCID 178446192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| Reactant | 1-Pentyl-6-methoxy-isatin | HCID 25194456 | — |
| Product | HCID 178446192 | HCID 178446192 | — |
Reaction Steps
The title compound was prepared as a yellow solid, using 1-pentyl-6-methoxy-isatin obtained in Example 39(A) and Phenylacetic hydrazide according to the synthetic method E. NMR (CDCl3): δ 0.91 (t, 3H), 1.33 to 1.39 (m, 4H), 1.66-1.69 (m, 2H), 3.62-3.76 (m, 2H), 3.85-3.88 (m, 3H), 4.14 and 4.23 (s for isomers, 1H), 6.38-6.64 (m, 2H), 7.22-7.26 (m1H), 7.32 (m, 2H), 7.38-7.39 (m, 1H), 7.42 (d, 1H), 7.54 and 7.56 (d for isomers, 1H), 9.25 and 12.44 and 12.99 (br s for isomers, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309595B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-5ce3f6a39c824590bf3f1a669eeff8f2 |
| Source note | uspto-grants-2012_11 |