HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylbenzoic acid → HCID 24874979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylbenzoic acid | HCID 10194 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 68950908 | HCID 68950908 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 24874979 | HCID 24874979 | — |
Reaction Steps
50 mg of (11) as 2HCl salt and 1201l of DIPEA were dissolved in 1 ml of DMSO. 29 mg of the OAT ester of 2,4,6-trimethylbenzoic acid were added. The solution was stirred for 12 h and the product was purified by HPLC to give 10.8 mg of (12) as TFA salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309735B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-d0002379401c441eb7825e427e1434d0 |
| Source note | uspto-grants-2012_11 |